tag:blogger.com,1999:blog-8964719845369935777.post7412440237996393920..comments2024-03-27T21:23:40.339-04:00Comments on Chemjobber: Bonus Process Wednesday: small-scale agitation parametersChemjobberhttp://www.blogger.com/profile/15932113680515602275noreply@blogger.comBlogger1125tag:blogger.com,1999:blog-8964719845369935777.post-35121173243836172322013-02-20T15:42:54.646-05:002013-02-20T15:42:54.646-05:00It makes sense if the ultimate oxidant is air (alt...It makes sense if the ultimate oxidant is air (although you have plenty of silver carbonate). It slowly gets used up over time and you only have a 50mL tube. If it was possible to put a needle connected to an air cylinder at the bottom of the reaction and bubble it, maybe the result would have been better, but you can't really do that at 140C with DMF.<br /><br />At least the reaction works. IBX on the other hand? Well... uncle samnoreply@blogger.com