In this week's C&EN, this letter to the editor:
I just had to comment on the two pieces from Newscripts in the April 1 issue of C&EN (page 40). In the first piece, the revelation by Jessica Pomerantz reminded me of an experience I had in 1977 in a senior-level physical chemistry class at Iowa State University.
It involved a Lewis acid-base reaction of boron trifluoride and trimethylamine in a rather complex glass network that included a liquid-nitrogen cold trap because the reaction was so exothermic. The instructions for valve settings and operation were quite specific and stated that if they were not followed explicitly, the apparatus could explode. I arranged all valves meticulously, or so I thought, and then opened the valve on the BF3 cylinder, which was connected to the glassware inlet by a rubber hose. Unfortunately, the one valve I forgot to open was the inlet valve to the apparatus. Within seconds, the hose popped off, and I had a fuming ball of BF3 within 1 ft (0.3 m) or so of my face. I had the presence of mind to shut off the cylinder valve, and then I watched as the fuming cloud, which stayed intact, floated to the ceiling and rolled all the way to the other corner and escaped through a roof vent. It reminded me of the movie The Blob, except this blob rolled along the ceiling and not the floor. My classmates and the teaching assistant were so absorbed in their own work that they did not observe the blob. Nobody at Iowa State ever learned of my slight mistake. I successfully completed the experiment on the second attempt.
This brings me to the second Newscripts article. During my many years in industry and to this day, I have written numerous articles for various technical trade magazines, including Chemical Engineering, Power Engineering, and others. I am now a self-employed technical writer and consultant. From the experience above and several others during my career (such as tripping and falling into several inches of yucky flue gas desulfurization sludge), I can decidedly appreciate the title of the second piece, “And This Is Why We’re Journalists Now.”
Brad Buecker
Lawrence, Kansas
I've had my share of near misses and dumb errors and I'm glad that I can look at them with humor now.
It is strange to me how laboratory chemical experiments of the past were seemingly so complex compared to the microscale experiments I performed in my undergraduate education in the 1990s. While we certainly generated less waste, I wonder if some of the really cool chemistry was lost to time...
(The answer to the headline is, of course, "yes.")
Well my undergrad organic lab back in 1974 was pretty simple... We jut had to distill benzene... at the bench rather than in a hood!.
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